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Basics of SPETechnology & MechanismsPieter Grobler,Sigma-Aldrich RSA Agenda• The Importance of Sample Prep• Overview of SPE Technology• SPE Strategies• Understanding Retention Mechanismssigma-aldrich.com Analytical Chromatography Heaven• Short run times• Baseline resolution• Symmetric peak shape• Good S/N ratio• No misleading peaks• High precision/accuracysigma-aldrich.com The Importance...
Key words
spe, speiox, ioxsample, sampleelution, elutionionized, ionizedsolvent, solventsorbent, sorbentbind, bindtube, tubeanalytes, analytescommon, commonserological, serologicalphase, phasematrix, matrixdilute
Systematic SPE Method Development
2003|Merck|Technical notes
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoTechnical ReportSystematic SPE Method DevelopmentComparison of a systematically developed method using Discovery DSC-8 SPE 96-Well Plate vs.a generic method using conventional C18 for the extraction and HPLC...
Key words
diazepam, diazepamwhat, whatsystematically, systematicallyload, loadspe, speobjectives, objectivesanalyte, analytesample, samplemethod, methodprep, prepoptimal, optimalmetabolites, metabolitesmatrix, matrixmajor, majorhydrophobic
 

Similar PDF

Toggle
Basics of SPETechnology & MechanismsPieter Grobler,Sigma-Aldrich RSA Agenda• The Importance of Sample Prep• Overview of SPE Technology• SPE Strategies• Understanding Retention Mechanismssigma-aldrich.com Analytical Chromatography Heaven• Short run times• Baseline resolution• Symmetric peak shape• Good S/N ratio• No misleading peaks• High precision/accuracysigma-aldrich.com The Importance...
Key words
spe, speiox, ioxsample, sampleelution, elutionionized, ionizedsolvent, solventsorbent, sorbentbind, bindtube, tubeanalytes, analytescommon, commonserological, serologicalphase, phasematrix, matrixdilute
Systematic SPE Method Development
2003|Merck|Technical notes
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoTechnical ReportSystematic SPE Method DevelopmentComparison of a systematically developed method using Discovery DSC-8 SPE 96-Well Plate vs.a generic method using conventional C18 for the extraction and HPLC...
Key words
diazepam, diazepamwhat, whatsystematically, systematicallyload, loadspe, speobjectives, objectivesanalyte, analytesample, samplemethod, methodprep, prepoptimal, optimalmetabolites, metabolitesmatrix, matrixmajor, majorhydrophobic
 

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