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DEVELOPMENT OF A SPE LC-MS/MS METHOD FOR THEBIOANALYTICAL QUANTIFICATION OF PRAMLINTIDE FROM SERUMCaitlin M. Dunning, Mary E. Lame, Mark D. Wrona, Kim Haynes, and Ian EdwardsWaters Corporation, Milford, MA, USAINTRODUCTIONRESULTSScreening GradientOptimized Gradient15% gradient start15 – 60% B in 2 minutes20%...
Key words
pramlintide, pramlintideserum, serumrat, ratlqc, lqclloq, lloqquantification, quantificationspe, spehuman, humanstatistics, statisticsquanrecovery, quanrecoveryhqc, hqcmqc, mqcmaxpeak, maxpeakwcx, wcxuplc
Development of a SPE LC-MS/MS Method Utilizing QuanRecoverySample Plates with MaxPeak High Performance Surfaces for theBioanalytical Quantification of Pramlintide from SerumCaitlin Dunning, Mary Lame, Mark Wrona, and Kim HaynesWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■■■■■INTRODUCTIONWaters™ Oasis™ Peptide SeparationTechnologies (PST) µElution™ SPEscreening...
Key words
quanrecovery, quanrecoverypramlintide, pramlintidemaxpeak, maxpeakplates, platessurfaces, surfacesoasis, oasisasn, asnspe, spethr, thrserum, serumutilizing, utilizingwcx, wcxhigh, highuplc, uplclqc
A Rapid Method for the Ultra-Sensitive Quantification of FluticasonePropionate and Salmeterol Xinafoate from Human PlasmaNikunj Tanna, Lauren Mullin, and Robert PlumbWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■Ultra-sensitive quantificationFluticasone propionate (Figure 1A) 1 is a synthetic trifluorinatedof fluticasone propionate andglucocorticoid receptor agonist...
Key words
fluticasone, fluticasonesalmeterol, salmeterolxinafoate, xinafoatepropionate, propionateplasma, plasmaaccuracy, accuracyquantification, quantificationhuman, humaninter, interultra, ultrasensitive, sensitiveuplc, uplcday, dayrapid, rapidasthma
Development of a SPE LC-MS/MS Method for the BioanalyticalQuantification of Salmon Calcitonin from Human SerumNikunj Tanna and Mary LameWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■Sensitive and flexible platform forSalmon calcitonin (sCT) is a 32 amino acid (MW 3439.1 Da) syntheticquantification of...
Key words
calcitonin, calcitoninsalmon, salmonquantification, quantificationoasis, oasisspe, spebioanalytical, bioanalyticalserum, serumsct, sctwcx, wcxdevelopment, developmentrecovery, recoveryhuman, humanprotein, proteinprecipitation, precipitationxevo
 

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DEVELOPMENT OF A SPE LC-MS/MS METHOD FOR THEBIOANALYTICAL QUANTIFICATION OF PRAMLINTIDE FROM SERUMCaitlin M. Dunning, Mary E. Lame, Mark D. Wrona, Kim Haynes, and Ian EdwardsWaters Corporation, Milford, MA, USAINTRODUCTIONRESULTSScreening GradientOptimized Gradient15% gradient start15 – 60% B in 2 minutes20%...
Key words
pramlintide, pramlintideserum, serumrat, ratlqc, lqclloq, lloqquantification, quantificationspe, spehuman, humanstatistics, statisticsquanrecovery, quanrecoveryhqc, hqcmqc, mqcmaxpeak, maxpeakwcx, wcxuplc
Development of a SPE LC-MS/MS Method Utilizing QuanRecoverySample Plates with MaxPeak High Performance Surfaces for theBioanalytical Quantification of Pramlintide from SerumCaitlin Dunning, Mary Lame, Mark Wrona, and Kim HaynesWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■■■■■INTRODUCTIONWaters™ Oasis™ Peptide SeparationTechnologies (PST) µElution™ SPEscreening...
Key words
quanrecovery, quanrecoverypramlintide, pramlintidemaxpeak, maxpeakplates, platessurfaces, surfacesoasis, oasisasn, asnspe, spethr, thrserum, serumutilizing, utilizingwcx, wcxhigh, highuplc, uplclqc
A Rapid Method for the Ultra-Sensitive Quantification of FluticasonePropionate and Salmeterol Xinafoate from Human PlasmaNikunj Tanna, Lauren Mullin, and Robert PlumbWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■Ultra-sensitive quantificationFluticasone propionate (Figure 1A) 1 is a synthetic trifluorinatedof fluticasone propionate andglucocorticoid receptor agonist...
Key words
fluticasone, fluticasonesalmeterol, salmeterolxinafoate, xinafoatepropionate, propionateplasma, plasmaaccuracy, accuracyquantification, quantificationhuman, humaninter, interultra, ultrasensitive, sensitiveuplc, uplcday, dayrapid, rapidasthma
Development of a SPE LC-MS/MS Method for the BioanalyticalQuantification of Salmon Calcitonin from Human SerumNikunj Tanna and Mary LameWaters Corporation, Milford, MA, USAAPPLICATION BENEFITS■■■■Sensitive and flexible platform forSalmon calcitonin (sCT) is a 32 amino acid (MW 3439.1 Da) syntheticquantification of...
Key words
calcitonin, calcitoninsalmon, salmonquantification, quantificationoasis, oasisspe, spebioanalytical, bioanalyticalserum, serumsct, sctwcx, wcxdevelopment, developmentrecovery, recoveryhuman, humanprotein, proteinprecipitation, precipitationxevo
 

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