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The Effects of SFC Preparative Scale-up on Throughput, Purityand Recovery of an Impurity in an API MixtureCatharine Layton, Andrew Aubin, Jacquelyn Runco, Shawn HelmuellerWaters Corporation, Milford, MA, 01757, USAINTRODUCTIONScale-up of SFC analytical methods to preparative scale allowslaboratories to generate purified...
Key words
hour, hourcost, costper, perpurity, puritycosolvent, cosolventscale, scalecycle, cyclepreparative, preparativethroughput, throughputstock, stockisolate, isolateapi, apiobserved, observedanalytical, analyticalsfc
THE EFFECTS OF SFC PREPARATIVE SCALE-UP ONTHROUGHPUT, PURITY AND RECOVERY OF AN IMPURITYIN AN API MIXTURECatharine Layton1, Andrew Aubin1, Jacquelyn Runco1, Shawn Helmueller1, Charlotte Yu2, Nobutake Sato31Waters Corporation, Milford, MA, 01757, USA, 2Waters Asia Headquarters, Seoul, Korea, 3Waters Asia Headquarter,...
Key words
hour, hourcost, costscale, scalepreparative, preparativeper, perpurity, purityhput, hputcycle, cyclethroug, througstock, stockisolate, isolatesfc, sfcanalytical, analyticaldesired, desiredobserved
A Comparative Study Using Preparative Reverse Phase LiquidChromatography and Supercritical Fluid Chromatography ofImpurities from a Stressed Pharmaceutical Drug SubstanceJanet Hammond, 1 Russell Mortishire-Smith, 1 Jayne Kirk,1 and Christopher Howson 2,3Waters Corporation, Wilmslow, United Kingdom; 2 Syngenta UK Ltd Jealott’s Hill...
Key words
sfc, sfcpreparative, preparativesupercritical, supercriticaltorus, torusacquity, acquityfluid, fluidcomparative, comparativereverse, reversechromatography, chromatographyphase, phaseqda, qdaimpurities, impuritiesuplc, uplcpurification, purificationdryness
Enantioseparation of Metalaxyl Using ACQUITY UPC 2 and Small-ScalePurification Using the Investigator SFC SystemJohn McCauley, Jaci Runco, and Marian TwohigWaters Corporation, Milford, MA, USAA P P L I C AT I O N B E N E F I T...
Key words
sfc, sfcchiral, chiralinvestigator, investigatorpreparative, preparativestacked, stackedpurification, purificationenantiomers, enantiomersadhering, adheringchromatography, chromatographyacquity, acquityshorter, shorterscale, scalelarger, largerstrict, strictrun
 

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The Effects of SFC Preparative Scale-up on Throughput, Purityand Recovery of an Impurity in an API MixtureCatharine Layton, Andrew Aubin, Jacquelyn Runco, Shawn HelmuellerWaters Corporation, Milford, MA, 01757, USAINTRODUCTIONScale-up of SFC analytical methods to preparative scale allowslaboratories to generate purified...
Key words
hour, hourcost, costper, perpurity, puritycosolvent, cosolventscale, scalecycle, cyclepreparative, preparativethroughput, throughputstock, stockisolate, isolateapi, apiobserved, observedanalytical, analyticalsfc
THE EFFECTS OF SFC PREPARATIVE SCALE-UP ONTHROUGHPUT, PURITY AND RECOVERY OF AN IMPURITYIN AN API MIXTURECatharine Layton1, Andrew Aubin1, Jacquelyn Runco1, Shawn Helmueller1, Charlotte Yu2, Nobutake Sato31Waters Corporation, Milford, MA, 01757, USA, 2Waters Asia Headquarters, Seoul, Korea, 3Waters Asia Headquarter,...
Key words
hour, hourcost, costscale, scalepreparative, preparativeper, perpurity, purityhput, hputcycle, cyclethroug, througstock, stockisolate, isolatesfc, sfcanalytical, analyticaldesired, desiredobserved
A Comparative Study Using Preparative Reverse Phase LiquidChromatography and Supercritical Fluid Chromatography ofImpurities from a Stressed Pharmaceutical Drug SubstanceJanet Hammond, 1 Russell Mortishire-Smith, 1 Jayne Kirk,1 and Christopher Howson 2,3Waters Corporation, Wilmslow, United Kingdom; 2 Syngenta UK Ltd Jealott’s Hill...
Key words
sfc, sfcpreparative, preparativesupercritical, supercriticaltorus, torusacquity, acquityfluid, fluidcomparative, comparativereverse, reversechromatography, chromatographyphase, phaseqda, qdaimpurities, impuritiesuplc, uplcpurification, purificationdryness
Enantioseparation of Metalaxyl Using ACQUITY UPC 2 and Small-ScalePurification Using the Investigator SFC SystemJohn McCauley, Jaci Runco, and Marian TwohigWaters Corporation, Milford, MA, USAA P P L I C AT I O N B E N E F I T...
Key words
sfc, sfcchiral, chiralinvestigator, investigatorpreparative, preparativestacked, stackedpurification, purificationenantiomers, enantiomersadhering, adheringchromatography, chromatographyacquity, acquityshorter, shorterscale, scalelarger, largerstrict, strictrun
 

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